| dc.rights.license | In Copyright | en_US |
| dc.creator | Bramley, Michael Laird | |
| dc.date.accessioned | 2023-04-21T19:30:22Z | |
| dc.date.available | 2023-04-21T19:30:22Z | |
| dc.date.created | 1969 | |
| dc.identifier | WLURG038_Bramley_thesis_1969 | |
| dc.identifier.uri | https://dspace.wlu.edu/handle/11021/36166 | |
| dc.description | The title page of this thesis indicates that it was presented "in partial fulfillment of the requirements for the Bachelor of Science degree in Chemistry." | en_US |
| dc.description.abstract | The synthesis of [delta]9,10 octal-1-one has been begun in large quantities. The intermediate , methyl-[gamma]-(1-cyclohexenyl)-[gamma]-oxobutyrate has been obtained in workable amounts. A study of the use of semicarbazones and thiosemicarbazones in a modified Huang-Minlon reduction has been completed with the following results: the semicarbazones give the higher yields, the purer products, which are easier to clean up. It is suggested that the Huang-Minlon Reduction be continued on the methyl ester semicarbazone, and that it be refluxed with the KOH for the full 24 hours . [From Summary] | en_US |
| dc.format.extent | 21 pages | en_US |
| dc.language.iso | en_US | en_US |
| dc.rights | This material is made available for use in research, teaching, and private study, pursuant to U.S. Copyright law. The user assumes full responsibility for any use of the materials, including but not limited to, infringement of copyright and publication rights of reproduced materials. Any materials used should be fully credited with the source. | en_US |
| dc.rights.uri | http://rightsstatements.org/vocab/InC/1.0/ | en_US |
| dc.title | An Investigation of the Synthesis of [delta]9,10 Octal-1-one | |
| dc.type | Text | en_US |
| dcterms.isPartOf | WLURG38 - Student Papers | |
| dc.rights.holder | Bramley, Michael Laird | |
| dc.subject.fast | Chemistry, Organic | en_US |
| dc.subject.fast | Propellanes | en_US |
| dc.subject.fast | Thiosemicarbazones | en_US |
| local.department | Chemistry | en_US |
| local.scholarshiptype | Bachelor of Science | en_US |
